E-postama gönder EFFECT OF HF ACID ON THE FORMATION OF NEW 2D Ti3C2 MXENE FROM Ti3SiC2
Öz
EFFECT OF HF ACID ON THE FORMATION OF NEW 2D Ti3C2 MXENE FROM Ti3SiC2
Abstract
With the developing technology, our need for renewable energy also increases. Limited energy sources brought along our need for alternative energy sources. When layer A in MAX phases is scraped to highlight the similarity to graphene called MXene a new 2D material type is created. Studies on 2D materials are carried out by researchers in many areas from energy to health. Converted to rechargeable materials to meet energy needs Mxene has become a new energy storage material with its layered structure. With the etching of Ti3SiC2 powder in MAX phase with Hydrofluoric Acid (HF), it becomes an accordion-like two-dimensional Ti3C2 Mxene structure. Hydrofluoric Acid etching is the most used method in converting MAX phase to Mxene structure. Like conductivity properties of 2D materials determining and changing many features surface terminations such as -O, -OH, -F group on Mxene were effective. The Mxene structure is an extraordinary combination of electrical and mechanical properties that combine the properties of metals and ceramics. In this article, the effect of etching time with hydrofluoric acid is investigated. Mxene phase Ti3C2Tx powder subjected to hydrofluoric acid (HF) at room temperature for 2, 8, 16, 32, and 48 hours, X-ray diffraction (XRD) was analyzed by scanning electron microscopy (SEM & FESEM) and Brunauer-Emmett-Teller (BET) Theory.
Keywords: MAX phase, Mxene, Ti3SiC2, Hydrofluoric Acid, 2D Material
HF ASİDİNİN Ti3SiC2'DEN YENİ 2D Ti3C2 MXENE OLUŞUMU ÜZERİNDEKİ ETKİSİ
Özet
Gelişen teknoloji ile birlikte yenilenebilir enerji ihtiyacımız da artıyor. Sınırlı enerji kaynakları, alternatif enerji kaynaklarına olan ihtiyacımızı da beraberinde getirdi. MAX fazındaki A katmanı, MXene adı verilen grafene benzerliği vurgulamak için kazındığında yeni bir 2D malzeme türü oluşturulur. 2D malzemelerle ilgili çalışmalar, enerjiden sağlığa pek çok alanda araştırmacılar tarafından yürütülmektedir. Enerji ihtiyacını karşılamak için şarj edilebilir malzemelere dönüştürülen MXene, katmanlı yapısı ile yeni bir enerji depolama malzemesi haline geldi. Hidroflorik Asit (HF) ile Ti3SiC2 tozunun MAX fazında aşındırılmasıyla akordeon benzeri iki boyutlu Ti3C2 MXene yapısı haline gelir. Hidroflorik Asit aşındırma, MAX fazını MXene yapısına dönüştürmede en çok kullanılan yöntemdir. MXene üzerinde -O, -OH, -F grubu gibi birçok özellik yüzey sonlandırmalarını belirleyen ve değiştiren 2D malzemelerin iletkenlik özellikleri gibi etkili oldu. MXene yapısı, metallerin ve seramiğin özelliklerini birleştiren olağanüstü bir elektriksel ve mekanik özellik kombinasyonudur. Bu yazıda hidroflorik asit ile aşındırma süresinin etkisi araştırılmıştır. 2, 8, 16, 32 ve 48 saat boyunca oda sıcaklığında hidroflorik aside (HF) tabi tutulan MXene faz Ti3C2Tx tozu, X-ışını kırınımı (XRD) taramalı elektron mikroskobu (SEM & FESEM) ve Brunauer-Emmett-Teller (BET) Teorisi ile analiz edildi.
Anahtar Kelimeler: MAX faz, MXene, Ti3SiC2, Hidroflorik Asit, 2D Malzeme
Anahtar Kelimeler
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